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Atmospheric Plasma-Assisted Preparation of Graphene Oxide from Biomass: Characterization and Elemental Analysis


 
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1. Title Title of document Atmospheric Plasma-Assisted Preparation of Graphene Oxide from Biomass: Characterization and Elemental Analysis
 
2. Creator Author's name, affiliation, country A. H. Handayani; 1. Master Program in Nuclear Science and Engineering, Bandung Institute of Technology, Indonesia 2. Research Center for Nuclear Beam Analysis Technology, National Research and Innovation Agency, KST BJ Habibie, Serpong; Indonesia
 
2. Creator Author's name, affiliation, country F. Amalia; Research Center for Nuclear Beam Analysis Technology, National Research and Innovation Agency, KST BJ Habibie, Serpong; Indonesia
 
2. Creator Author's name, affiliation, country E. V. Noviantana; Directorate of Nuclear Power Facility Management, National Research and Innovation Agency, KST BJ Habibie, Serpong, Indonesia; Indonesia
 
2. Creator Author's name, affiliation, country T. R. Mulyaningsih; Research Center for Nuclear Beam Analysis Technology, National Research and Innovation Agency, KST BJ Habibie, Serpong; Indonesia
 
2. Creator Author's name, affiliation, country A. Waris; Master Program in Nuclear Science and Engineering, Bandung Institute of Technology, Bandung; Indonesia
 
2. Creator Author's name, affiliation, country A. Dimyati; Directorate of Laboratory Management, Research Facilities, and Science and Technology Park, National Research and Innovation Agency, KST Soekarno, Cibinong; Indonesia
 
3. Subject Discipline(s)
 
3. Subject Keyword(s) Graphene oxide; Atmospheric Plasma; NAA; SEM-EDS; Biomass; Raman spectroscopy
 
4. Description Abstract Graphene oxide (GO) was successfully synthesized using the atmospheric plasma process with biomass precursors, including coconut fronds, palm fronds, and rambutan stems, within a five-minute processing time. Plasma technology converts near-waste materials into valuable resources with potential for various applications. Graphene oxide, in particular, exhibits high mechanical strength, excellent electrical conductivity, good biocompatibility, and a large surface area, making it a highly versatile material. Raman spectroscopy was used to analyze the formation of synthesized graphene. The presence of organic and inorganic elements in graphene oxide was characterized using a scanning electron microscope equipped with energy-dispersive X-ray spectroscopy (SEM-EDS) and neutron activation analysis (NAA). SEM-EDS analysis revealed that the C:O ratio in plasma-derived graphene oxide exceeded 80 % in each sample. NAA identified 22 inorganic elements, which are naturally present in biomass. Understanding the elemental composition of plasma-synthesized graphene oxide is essential for evaluating its potential applications and identifying necessary purification steps. The oxygen content in the synthesized material, which primarily originates from the inherent properties of biomass, can be regulated by optimizing plasma parameters. Using biomass precursors makes plasma-synthesized graphene oxide an economically viable option for large-scale production.
 
5. Publisher Organizing agency, location National Research and Innovation Agency
 
6. Contributor Sponsor(s) The authors would like to thank Nuclear Power Research Organization (ORTN) for its financial support. The authors acknowledge the facilities, scientific and technical support from Neutron Scattering Laboratory and Research Nuclear Reactor G. A. Siwabessy,
 
7. Date (YYYY-MM-DD) 2025-04-14
 
8. Type Status & genre Peer-reviewed Article
 
8. Type Type
 
9. Format File format PDF
 
10. Identifier Uniform Resource Identifier https://atomindonesia.brin.go.id/index.php/aij/article/view/1472
 
10. Identifier Digital Object Identifier (DOI) https://doi.org/10.55981/aij.2025.1472
 
11. Source Title; vol., no. (year) Atom Indonesia; Vol 51, No 2 (2025): AUGUST 2025
 
12. Language English=en en
 
14. Coverage Geo-spatial location, chronological period, research sample (gender, age, etc.)
 
15. Rights Copyright and permissions Copyright (c) 2025 Atom Indonesia
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